"Establishment and Application of New Measuring Technology for O
「"Establishment and Application of New Measuring Technology for O」於資料集「EPQSummary_EnvironmentalMonitoringAndTesting」由單位「行政院環境保護署」的陳先生所提供，聯繫電話是02-2311-7722#2386，最近更新時間為：2023-07-30 01:01:45。 欄位Project Title的內容是"Establishment and Application of New Measuring Technology for Oil Pollution Identification（2/2）" ， 欄位Project Subject的內容是"One-dimensional gas chromatography method such as GC-FID or GC-MS for the analysis of samples resolution and peak capacity has its limits; especially for the unresolved complex mixtures (UCMs). For example, the co-elution phenomenon has occurredduring the oil analysis resolution separation process. Two-dimensional gas chromatography technique is proposed by using the two different polar or property columns to overcome the co-elution problem. This project is to establish and develop the comprehensive GCGC-TOFMS techniques and employ mass spectrometer assist GC for forensic analysis of biomarkers and their forensic applicable feasibility investigation.
The report has collected 20 literature surveys of a two-dimensional gas chromatography mass spectrometry and related oil pollution fingerprint forensic data, meanwhile, converge domestic and international oil pollution aggregated data and fingerprint forensic and technical reports, and completes the [Oil pollution forensic guidelines and case analysis - chemical characteristics of forensic Technical Manual (Draft)]. On the side of GCGC-TOFMS analysis conditions established, applied 2 imported samples of crude oil and 4 diesel samples provided by EAL’s 98s project to establish analytical conditions, instrument linear analysis, and precision (reproducibility analysis). The biomarker fingerprint and TIC of crude oil and diesel fuel have established by utilizing NIST database compared with TOFMS spectrum and standard spectra with relevant literatures.
The GCxGC-TOFMS oil pollution forensic applicability investigation has completed by calculate the ratio of the sum of the diagnosis which is provided by GC-MS biomarker resultsfrom differentiation and association of 2 crude oil samples (established by 98ys). In order to build an applicability GCxGC-TOFMS analysis verified, the differentiation of 8 crude oil samples had compared. The analytic results indicate that GCxGC-TOFMS and GC-MS present similar fingerprint, which mean the samples can be identified by carbon number distribution, biomarkers and diagnostic odds with the source characteristics and formation characteristics. The calculated rations of diagnosis are presented differences as the differentiation of instrument properties between GC-MS and GCxGC-TOFMS. However, the source characteristic can be recognized by both MS. It shows that the GCxGC-TOFMS analysis is an applicability of analytic technology. The GCxGC-TOFMS analysis technique has been proved the ability to distinguish between different types of oil from two real oil pollution cases.
The GCxGC-TOFMS has better separation factor and less co-elution phenomenon compare with GC-MS under more complex composition (such as crude oil), or a low content of biomarker samples conditions. Particularly for alkyl PAHs fingerprint sample, the GCxGC-TOFMS has given high distinguish, selectivity and separation of interfering compounds." ， 欄位Project Year的內容是2014 ， 欄位Organizer的內容是"Environmental Analysis Laboratory" ， 欄位Executive Unit的內容是"工業技術研究院" ， 欄位Reporting download URL的內容是https://epq.epa.gov.tw/project/filedownload.aspx?fid=73626 ， 欄位Publish Date的內容是20150201 。
Project Title
"Establishment and Application of New Measuring Technology for Oil Pollution Identification（2/2）"
Project Subject
"One-dimensional gas chromatography method such as GC-FID or GC-MS for the analysis of samples resolution and peak capacity has its limits; especially for the unresolved complex mixtures (UCMs). For example, the co-elution phenomenon has occurredduring the oil analysis resolution separation process. Two-dimensional gas chromatography technique is proposed by using the two different polar or property columns to overcome the co-elution problem. This project is to establish and develop the comprehensive GCGC-TOFMS techniques and employ mass spectrometer assist GC for forensic analysis of biomarkers and their forensic applicable feasibility investigation. The report has collected 20 literature surveys of a two-dimensional gas chromatography mass spectrometry and related oil pollution fingerprint forensic data, meanwhile, converge domestic and international oil pollution aggregated data and fingerprint forensic and technical reports, and completes the [Oil pollution forensic guidelines and case analysis - chemical characteristics of forensic Technical Manual (Draft)]. On the side of GCGC-TOFMS analysis conditions established, applied 2 imported samples of crude oil and 4 diesel samples provided by EAL’s 98s project to establish analytical conditions, instrument linear analysis, and precision (reproducibility analysis). The biomarker fingerprint and TIC of crude oil and diesel fuel have established by utilizing NIST database compared with TOFMS spectrum and standard spectra with relevant literatures. The GCxGC-TOFMS oil pollution forensic applicability investigation has completed by calculate the ratio of the sum of the diagnosis which is provided by GC-MS biomarker resultsfrom differentiation and association of 2 crude oil samples (established by 98ys). In order to build an applicability GCxGC-TOFMS analysis verified, the differentiation of 8 crude oil samples had compared. The analytic results indicate that GCxGC-TOFMS and GC-MS present similar fingerprint, which mean the samples can be identified by carbon number distribution, biomarkers and diagnostic odds with the source characteristics and formation characteristics. The calculated rations of diagnosis are presented differences as the differentiation of instrument properties between GC-MS and GCxGC-TOFMS. However, the source characteristic can be recognized by both MS. It shows that the GCxGC-TOFMS analysis is an applicability of analytic technology. The GCxGC-TOFMS analysis technique has been proved the ability to distinguish between different types of oil from two real oil pollution cases. The GCxGC-TOFMS has better separation factor and less co-elution phenomenon compare with GC-MS under more complex composition (such as crude oil), or a low content of biomarker samples conditions. Particularly for alkyl PAHs fingerprint sample, the GCxGC-TOFMS has given high distinguish, selectivity and separation of interfering compounds."
Project Year
2014
Organizer
"Environmental Analysis Laboratory"
Executive Unit
"工業技術研究院"
Reporting download URL
Publish Date
20150201
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