Development of Analytical Method for Organotins in Effluent2022
「Development of Analytical Method for Organotins in Effluent2022」於資料集「EPQSummary_ChemicalSubstanceManagement」由單位「行政院環境保護署」的陳先生所提供，聯繫電話是02-2311-7722#2386，最近更新時間為：2023-07-30 01:01:48。 欄位Project Title的內容是Development of Analytical Method for Organotins in Effluent ， 欄位Project Subject的內容是In this project, literatures related to the analysis technologies of organotin were reviewed. Also, analytical parameters of dibutyltin dilaurate and dibutyltin dichloride in LC/MS/MS were confirmed and chromatographic conditions and calibration curve were established. Quality control requirements of dibutyltin dilaurate and dibutyltin dichloride analysis method in the outfall water were also established. The method detection limits of the dibutyltin dilaurate and dibutyltin dichloride are 0.853 and 0.212 μg/L, respectively, which meet the requirements of the law enforcement. Requirements for the estimated concentration of the disclosed organotin discharge waste water pollutants. Three kinds of instrument tests have been completed in the announcement of toxic substances, including Pyr-GC/MS, GC/MS, and LC/MS/MS. Recommends were made that the toxic substances analysis can be preliminarily characterized by EGA mode of Py-GC/MS, and then by LC /MS/MS quantification, avoids sample derivatization procedures, and can simultaneously analyze organotin compounds such as butyltin,
triphenyltin chloride and tripropyltin chloride.
Since the organotin compound is a coordination compound, the original bonding group to the metal will be easily substituted. When the sample contains more than two kinds of organotin compounds with the same butyl group, it is easy to cause a qualitative misjudgment. After some modification, tributyltin, triphenyltin chloride and tripropyltin chloride can be simultaneously analyzed with liquid chromatography tandem mass spectrometer. It is recommended to follow strategies in other countries for the management of organotin, and evaluate the toxicity by sum of organotin homologues with same number of branch to avoid problems such as misjudgment caused by matrix effect in analysis. ， 欄位Project Year的內容是2022 ， 欄位Organizer的內容是 ， 欄位Executive Unit的內容是財團法人工業技術研究院 ， 欄位Reporting download URL的內容是https://epq.epa.gov.tw/ProjectDoc/FileDownload?fid=288271&proj_id=1110212969&doc_kind=1 ， 欄位Publish Date的內容是20230217 。
Project Title
Development of Analytical Method for Organotins in Effluent
Project Subject
In this project, literatures related to the analysis technologies of organotin were reviewed. Also, analytical parameters of dibutyltin dilaurate and dibutyltin dichloride in LC/MS/MS were confirmed and chromatographic conditions and calibration curve were established. Quality control requirements of dibutyltin dilaurate and dibutyltin dichloride analysis method in the outfall water were also established. The method detection limits of the dibutyltin dilaurate and dibutyltin dichloride are 0.853 and 0.212 μg/L, respectively, which meet the requirements of the law enforcement. Requirements for the estimated concentration of the disclosed organotin discharge waste water pollutants. Three kinds of instrument tests have been completed in the announcement of toxic substances, including Pyr-GC/MS, GC/MS, and LC/MS/MS. Recommends were made that the toxic substances analysis can be preliminarily characterized by EGA mode of Py-GC/MS, and then by LC /MS/MS quantification, avoids sample derivatization procedures, and can simultaneously analyze organotin compounds such as butyltin, triphenyltin chloride and tripropyltin chloride. Since the organotin compound is a coordination compound, the original bonding group to the metal will be easily substituted. When the sample contains more than two kinds of organotin compounds with the same butyl group, it is easy to cause a qualitative misjudgment. After some modification, tributyltin, triphenyltin chloride and tripropyltin chloride can be simultaneously analyzed with liquid chromatography tandem mass spectrometer. It is recommended to follow strategies in other countries for the management of organotin, and evaluate the toxicity by sum of organotin homologues with same number of branch to avoid problems such as misjudgment caused by matrix effect in analysis.
Project Year
2022
Organizer
Executive Unit
財團法人工業技術研究院
Reporting download URL
https://epq.epa.gov.tw/ProjectDoc/FileDownload?fid=288271&proj_id=1110212969&doc_kind=1
Publish Date
20230217
「Development of Analytical Method for Organotins in Effluent2022」所屬的資料集：「EPQSummary_ChemicalSubstanceManagement」的其他資料
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